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CHEN90012, Design and Construction of Equipment, Major Assignment 2024

S2.

Note the assignments of this year is substantially different from past. Comprehend the

description of the question with caution as follows:

Overview

1. This assignment makes up 60% of the total marks for PED. You must achieve 50% or more on

this assignment to pass the subject.

2. This assignment is due in three parts

Part 1 is due on 21 Aug at 5 PM. (20 marks)

Part 2 is due on 18 Sep at 5 PM. (25 marks)

Part 3 is due on 16 Oct at 5 PM. (15 marks)

If the assignment is late the following penalties will apply

Turned in on the following morning before 10AM: -5% of total marks for that part of

assignment.

Turned in on the following day before 5PM: -10% of total marks for that part of

assignment.

Turned in five days late: -50% of total marks for that part of assignment.

3. Each individual must make their own submission by the deadline.

(a) Submit your overall report including text, calculations or drawing together via Turnitin.

Make sure all your drawings are following the guidelines for “mechanical drawing” as

provided in the additional resources in LMS.

Generate your 2D drawing using an appropriate software (e.g. MS Visio or AutoCAD)

rather than do it in manual, and generate 3D drawing using AutoCAD 3D, SketchUp or

similar for 3D objects required in the assignment.

Original files of the 3D drawing must be uploaded in a separate file.

(b) Submit your calculation toll in a single sheet Excel spreadsheet in the format of Excel

Worksheet .xlsx or .xls to a secondary Turnitin portal and name your Excel spread sheet

in your own name and student number, e.g.

John Smith_123456_Assignment 1

For Excel sheet, you can refer to the guidelines given in the lecture note on “Calculation

Tools” but DO NOT COPY the note.

The Excel sheet must be clear, logical, and working!

4. Bonus marks

Bonus marks of 1.5 are applicable to each assignment.

Submissions that demonstrate original critical thinking and exceptional quality of design

will be considered for bonus marks.

You are allowed to discuss your design with your fellow students but:

1

You cannot use the same spread sheet as another student.

You cannot submit the same text, calculations or drawing as another student.

You must submit only your own work.

5. Plagiarism and other matters

The definitions of Plagiarism and Collusion and their consequences are outlined in the

coversheet that you must sign. Keep a copy of your assignment; you will need it to start

parts 2 and 3 even before the previous part is returned to you.

The whole report should be written by Calibri style with font 12 for the whole text and 14

bold for headings, equipment labels of 10 bold, and 1.5 line space.

6. This is an individual assignment

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The Design Problem

Aggressive measures need to be taken to address the greenhouse gas emissions in hard-to-

abate industries, such as marine shipping and aviation. Air-to-fuel has been identified as a potential

pathway to produce carbon-neutral or carbon-negative chemical fuels from air components and

renewable energy.

Here, you are leading the design of an air-to-fuel plant with a daily production rate of 200

ton methanol (based on pure MeOH). A direct air capture (DAC) unit (denoted as D1 for flowsheet)

based on amine scrubbing has been selected to produce high purity CO from air. Assuming 50%

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capture efficiency, and 500 ppm CO in the atmosphere, the gases CO produced by the stripper is

2 2

pressurized by a compressor (C1) to 3 MPa and stored in buffer tanks (T1) at ambient temperature

for the next step process.

A water splitting unit operating at ambient pressure has been selected to produce high purity

hydrogen gas. The Faradaic efficiency towards H and current efficiency of the electrolyser (E1) is

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100%, and 65% (i.e. 35% energy loss by joule heat), respectively. The electrolyser temperature

must be kept in the working range of 80 – 95 °C which is achieved by removing around 85% of the

joule heat by active cooling. Hot electrolyte (30% KOH aqueous solution) at 95 °C bleeds from one

end of the electrolyser and feeds to a heat exchanger (HE1); after cooling to 80 °C by ambient

running water, the electrolyte is mixed with 80 °C makeup water re-enters the electrolyser from the

other end. The product H is pressurized by a compressor (C2) to 3 MPa and stored in tanks (T2)

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temporarily for subsequent processes.

The aforementioned H and CO gas at 3MPa are mixed at 3:1 ratio (v/v) and stored in tanks

2 2

(T3). The mixed gas is then directed to a multi-cycle catalyser operating at 250 °C at 30 MPa to

produce methanol, via the following reaction:

3H + CO == CH OH + H O (1)

2 2 3 2

For practical purpose, 100% conversion of the raw gas and 100% MeOH selectivity are

assumed. The products are fully condensed by a heat exchanger (HE2) to produce liquid MeOH and

H O. A distillation unit (D1) is employed to enrich the MeOH to 99% in the distillate while the

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residue should contain no more than 1% MeOH.

The final product MeOH is stored in ambient tanks (T4) and shipped by trucks for sale.

The DAC and the catalyser are running continuously 24/7. Due to the intermittent nature of

solar energy, the water electrolyser is powered by compatible solar power facility during the

daytime and there is no power supply to the electrolyser during the nighttime.

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Provide design specifications and equipment drawings for the following pieces of

equipment:

(1) tank T2

(2) heat exchanger HE1, and

(3) distillation tower D1

The design specifications must follow the step-by-step calculations as shown during the

examples done in class following the outline in the lecture notes. For each piece of equipment you

must include:

1) a maximum one page executive summary

2) an equipment specification sheet

3) the detailed design calculations and discussion stating assumptions used in the

calculations. (Follow the Calculation Tools to make clear and legible calculations, or see

specific requirements of the individual assignments)

4) an engineering drawing of the equipment.

5) a 3D drawing of the equipment. (or see specific requirements of the individual

assignments)

5) description of the managerial, operational procedures and safety considerations for each

piece of equipment. Explain how all rules and regulations of the statutory authorities are

met.

6) references used for the design (must use Harvard style).

Marks will be deducted if the submission is not clear and legible or if the information is not

presented in an organised and logical manner. Demonstration of original thinking will be required

in order to gain full marks or even bonus. Some template of equipment specification sheet on

Canvas may not represent perfect example, and exact copying of that template will compromise

your marks.

Propose a reasonable equipment layout. The storage tanks should be located at least 100m

from other units of operation. The flash drum and heat exchanger can be placed between 40 to 50m

from the distillation tower. A process flow sheet and equipment layout (plan view) drawings of the

entire plant are also required.

Design data such as physical properties of the liquids and gasses can be found using Hysys,

Aspen, or in Perry’s Chemical Engineers Handbook and C&R Vol. 6 for example. The benzene-1-

pentanol VLE data are attached at the end of this assignment sheet. Steam at a maximum pressure

of 6 atm and utility water (returned from an evaporative cooling tower) at 15°C are available.

Marking rubric available on LMS.

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CHEN90012, Major Assignment 2024 S2.

Part 1

This part of the assignment makes up 20% of the total marks for PED.

Part 1 is due on 21 Aug at 5 PM. (20 marks)

Maximum 40 pages for text, calculations or drawing.

Provide design specifications and equipment drawings for the storage tanks (T2). Include details

about inlet and outlet nozzles etc. also a sketch of the tank farm layout.

The submission should include the following sections:

1). Report for overall design

a. Executive Summary 4% of total marks

b. Equipment Specification Sheet 15% of total marks

c. Process Flow Sheet and mass balance for the entire plant. 10% of total marks

c. Equipment Drawings 2D 20% of total marks

d. Detailed Calculations and Discussion 30% of total marks

e. Managerial Aspects (safety, operation, compliance, etc.) 5% of total marks

f. References (List & Appendices) 1% of total marks

2. Calculation Tool (Excel sheet) 15% of total marks

The Calculations and Discussion must be clearly legible. The Discussion should include

assumptions, justifications, procedures and conclusions from Calc. Tool design. The Managerial

Aspects should include any safety issues, operational and managerial issues, compliance with

regulations etc.

3). 3D drawing - optional - up to 5% bonus

Up to 10% of the marks will be based on evaluation of the writing (structure, readability, grammar

and Figures) and originality of the submission.

Submissions that demonstrate original critical thinking and exceptional quality of design will be

considered for bonus marks.

Remember to keep a copy of your submission so that you can work on the following part even

before this part is returned back marked.

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CHEN90012, Major Assignment 2024 S2.

Part 2

This part of the assignment makes up 25% of the total marks for PED.

Part 2 is due on 18 Sep at 5 PM.

Maximum 40 pages.

(25 marks)

Provide design specifications and equipment drawings for a shell-and-tube heat exchanger (HE1).

Note the cooling utility water should not exit the heat exchanger at more than 50oC. You must show

the step by step design, as in the example, but may use output from Hysys to validate your

calculations. (20 marks).

The submission should include the following sections:

1. Report for overall design

a. Executive Summary 4% of total marks

b. Equipment Specification Sheet 15% of total marks

c. Equipment Drawings 20% of total marks

d. Detailed Calculations and Discussion 30% of total marks

e. Managerial Aspects (safety, operation, compliance, etc.) 5% of total marks

f. References (List & Appendices) 1% of total marks

2. Calculation Tool (Excel sheet) 15% of total marks

The Calculations and Discussion must be clearly legible. The Discussion should include

assumptions, justifications, procedures and conclusions from Calc. Tool design. The Managerial

Aspects should include any safety issues, operational and managerial issues, compliance with

regulations etc.

3. Original file of 3D equipment drawings. 10% of total marks

Level of details: apart from the external shell, you must show the 3D of the tube bundle (with tube

sheet on). You can choose to present the tube bundle as an internal part of the HEX. Or, you can

present the tube bundle separately side by side of the shell.

Up to 10% of the marks will be based on evaluation of the writing (structure, readability, grammar

and Figures) and originality of the submission.

Submissions that demonstrate original critical thinking and exceptional quality of design will be

considered for bonus marks.

Remember to keep a copy of your submission so that you can work on the following part even

before this part is returned back marked.

Hint: Use an Excel spreadsheet to do the calculations so that you can easily change parameters and

recalculate the flow rates, pressure drops, overall heat transfer coefficients etc more easily. Once

you have made a final selection of configuration, tube diameter, length, number etc. etc, then you

should write out the step by step calculations for that final design.

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Comparing and contrasting the advantages and disadvantages of more than one design will be

considered favourably.

7

CHEN90012, Major Assignment 2024 S2.

Part 3

This part of the assignment makes up 15% of the total marks for PED.

Part 3 is due on 16 Oct 5PM.

Maximum 50 pages.

(15 marks)

Provide design specifications and equipment drawings for the plate distillation tower (D1). You

must show the step by step design, as in the example, but may use output from Hysys or Distil to

validate your calculations. (15 marks).

The submission should include the following sections:

1. Report for overall design

a. Executive Summary 5% of total marks

b. Equipment Specification Sheet 10% of total marks

c. Equipment Drawings (2D) 20% of total marks

d. Plant Layout 5% of total marks

e. Detailed Calculations and Discussion 40% of total marks

f. Managerial Aspects (safety, operation, compliance, etc.) 5% of total marks

g. References (List & Appendices) 1% of total marks

h. Appendix: Provide a drawing of the plant layout (plan view) for the entire processing

facility.

14% of total marks

2. Original file of 3D equipment drawings. up to 5% bonus marks

The Calculations and Discussion must be clearly legible. The Discussion should include

assumptions, justifications, procedures and conclusions from Calc. Tool design. The Managerial

Aspects should include any safety issues, operational and managerial issues, compliance with

regulations etc.

Up to 10% of the marks will be based on evaluation of the writing (structure, readability, grammar

and Figures) and originality of the submission.

Submissions that demonstrate original critical thinking and exceptional quality of design will be

considered for bonus marks.

Remember to keep a copy of your submission so that you can work on the following part even

before this part is returned back marked.

Hint: Use an Excel spreadsheet to do the calculations so that you can easily change parameters and

recalculate the flow rates, pressure drops, back up heights, residence times, flooding, entrainment

etc. etc more easily. Once you have made a final selection of configuration, tray spacing and

layout, number and size of holes, column diameter etc. etc, then you should write out the step by

step calculations for that final design.

Comparing and contrasting the advantages and disadvantages of more than one design will be

considered favourably.

8

VLE data of MeOH-H2O can be found in literature.

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